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Pure Food Grade Glacial Acetic Acid - High Purity & Food Safe



Industry Applications, Technical Specifications, and Quality Standards

Introduction

Food grade glacial acetic acid (CH₃COOH) is a fundamental organic compound widely recognized as the primary component responsible for vinegar's distinctive sour taste and pungent aroma. As a designated acidity regulator (E260) in the food additive classification system, this highly purified form of acetic acid meets stringent safety requirements for consumption and food processing applications. With a concentration of 99-100%, glacial acetic acid solidifies at temperatures below 16.7°C, explaining its "glacial" nomenclature.

The global market for food grade glacial acetic acid is projected to reach $13.2 billion by 2028, growing at a CAGR of 5.7% from 2023 onward (Food Chemical News, 2023). This growth is fueled by increasing demand in food preservation, flavor enhancement, and pH adjustment applications across processed foods, condiments, and beverages. This guide explores technical specifications, industry applications, safety considerations, and quality standards essential for manufacturers and food processors.

Hebei Yishan Spices Co., Ltd.

Leading manufacturer of premium food grade glacial acetic acid meeting international quality standards. We specialize in producing high-purity acetic acid solutions for diverse food industry applications.

📞 Phone: +86 13930492327

📱 Mobile: +86 15003215644

✉️ Email: yishanxiangliao@163.com

🏢 Address: 200 meters northeast of the intersection of East Airport Road and Airport North Street, Zengcun Town, Shijiazhuang City, Hebei Province

🌐 Website: https://www.ysxlglacialaceticacid.com

Product Overview

Acetic acid, an organic compound belonging to the carboxylic acid family, is widely present in nature and recognized as the source of sourness and characteristic pungent odor in vinegar. In food-grade applications, glacial acetic acid (a 99-100% concentration) requires specialized production processes to achieve pharmaceutical and food safety standards. Food grade glacial acetic acid serves multiple functions:

  • Acidity regulator (E260) adjusting pH in food systems
  • Preservative inhibiting microbial growth in acidic environments
  • Flavor enhancer in condiments, dressings, and sauces
  • Chemical intermediate in food-grade additives manufacturing
  • Vinegar production through controlled dilution and fermentation

Our food grade glacial acetic acid undergoes triple-distillation purification processes to achieve 99.8-100% concentration with non-detectable heavy metals (lead, arsenic, mercury below 0.1 ppm) and meets stringent requirements outlined in Food Chemicals Codex (FCC) and JECFA specifications. Packaging includes specialized chemical-grade polyethylene container111s in 25kg, 200kg, and IBC tank (1000kg) configurations.

Technical Specifications

Our food grade glacial acetic acid exceeds international standards for purity and safety. Below are key technical parameters compared with industry benchmarks:

Parameter Industry Standard (FCC) Yishan Premium Grade Test Method
Assay (CH₃COOH) ≥99.5% 99.8-100.0% USP Titration
Appearance Clear, colorless liquid Clear, colorless liquid Visual Inspection
Freezing Point ≥14.8°C 15.6-16.7°C ASTM D852
Residue After Ignition ≤0.002% ≤0.001% USP 〈281〉
Heavy Metals (as Pb) ≤0.0002% USP 〈231〉
Formic Acid & Oxidizable Impurities Pass test Pass test (≤0.08%) USP 〈401〉
Chroma (Pt-Co scale) ≤10 ≤5 ASTM D1209
Permanganate Time ≥60 minutes ≥120 minutes GB/T 1628

Industry Applications

Food grade glacial acetic acid serves versatile functions in the food manufacturing sector:

1. Condiment Production

Diluted to 4-8% solutions as vinegar base for mustards, ketchup, mayonnaise, and salad dressings. Effective pH regulator extending shelf-life by creating unfavorable environment for spoilage microorganisms. The acidity level of food grade glacial acetic acid solutions effectively inhibits growth of E. coli and Salmonella at pH below 4.5 (Journal of Food Protection, 2022).

2. Bakery Preservation

0.1-0.3% concentration extends mold-free shelf life in bread and baked goods by 40-80% compared to conventional propionates (Baking Science & Technology, 2023).

3. Pickling & Fermentation

Standardizes acetic acid content at 0.5-2.0% in pickle brines ensuring consistent preservation effectiveness and flavor profile while inhibiting undesirable microflora.

4. Beverage Acidulation

Adjusts tartness in non-carbonated drinks and kombucha at 0.005-0.03% concentration while meeting FDA GRAS (Generally Recognized as Safe) requirements.

5. Dairy Product Processing

Precipitates casein proteins in cheese manufacturing through pH-driven isoelectric precipitation at precisely controlled concentrations.

Quality & Safety Standards

Food safety standards require food grade glacial acetic acid to meet stringent specifications beyond technical-grade acetic acid:

  • Compliance: FCC Grade, FDA 21 CFR, EU Regulation (EC) No 1333/2008, JECFA
  • Heavy Metal Limits: Arsenic ≤1 ppm, Lead ≤0.5 ppm, Mercury ≤0.1 ppm
  • Microbiological: Total Plate Count ≤100 CFU/ml, Yeast/Mold ≤10 CFU/ml
  • Residual Solvents: Methanol ≤50 ppm, Benzene ≤2 ppb (GC-MS testing)
  • Traceability: Lot-controlled production with Batch Certificates of Analysis

Proper handling requires chemical-resistant PPE including neoprene gloves, face shields, and vapor respirators when handling concentrated solutions due to corrosive properties (pH 2.4 at 1% concentration). Storage recommendations include dedicated chemical-compatible HDPE container111s at temperatures between 15-25°C in well-ventilated areas.

Request Certificate of Analysis

Professional FAQ

Q1: What distinguishes food grade glacial acetic acid from technical grade?
Food-grade acetic acid undergoes additional purification steps including molecular distillation, microfiltration, and rigorous metals testing to achieve USP/FCC specifications with ≤0.5ppm heavy metals, whereas technical-grade contains higher residual impurities and is unsuitable for consumption.
Q2: What is the crystallization point of glacial acetic acid?
Pure glacial acetic acid solidifies at 16.6°C (61.9°F) due to hydrogen bonding. Industry specifications require minimum freezing points of 14.8°C (FCC) and 15.6°C for premium grades. Crystallization indicates high purity with low water content.
Q3: How do JECFA specifications differ from FCC standards?
While both specify minimum 99.5% acetic acid content, JECFA includes additional testing for mercury (max 0.03mg/kg), whereas FCC requires permanganate reduction time ≥60 minutes. Our product exceeds both with 99.8% purity and permanganate time >120 minutes.
Q4: What container111 materials are compatible with glacial acetic acid?
Storage requires chemical-grade polyethylene (PE), polypropylene (PP), or stainless steel 316L container111s. Avoid carbon steel, aluminum, zinc, or copper which corrode rapidly. Concentrated acetic acid attacks PVC at >40°C. All our packaging uses FDA-approved HDPE container111s.
Q5: What concentration dilution provides optimal microbial control?
Preservative effectiveness occurs at concentrations >0.1% undissociated acid, corresponding to pH
Q6: How is glacial acetic acid produced to food-grade standards?
After initial methanol carbonylation, distillation processes achieve 99.7% concentration. Food-grade purification includes molecular sieves dehydration, micro-filtration to 0.2μm, catalytic oxidation of impurities, and UV-light sterilization to achieve USP/FCC standards.
Q7: What thermal decomposition concerns exist?
Above 150°C, thermal decomposition produces ketene (highly toxic) and carbon dioxide. Processing requires temperature control below 100°C. Ketene converts to acetic anhydride at 700°C, but food applications never approach these temperatures.

References:

1. Food Chemical Codex (FCC 12) - Acetic Acid, Glacial Monograph. https://www.foodchemicalscodex.org/

2. JECFA Specifications for Acetic Acid (2023). FAO JECFA Monographs 31. https://www.fao.org/food/food-safety-quality/scientific-advice/jecfa/en/

3. "Microbial Inhibition by Weak Acid Preservatives" - Journal of Food Protection (2022). https://meridian.allenpress.com/jfp

4. "Acetic Acid Applications in Food Processing" - Food Technology Magazine (2023). https://www.ift.org/news-and-publications/food-technology-magazine

5. Global Acetic Acid Market Analysis Report 2023-2028. https://www.foodchemicalnews.com


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